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SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.上海禹重实业有限公司为您提供分析仪，期待为您服务！原装分析仪厂家直销

Procedure-SolidSamples：--Instrumentcalibration/driftcorrection.Placethenickelbasketcontainingthecalibration/driftstandardintotheopenportatthetopoftheloadinghead.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.衢州LECO氧氮氢分析仪怎么样上海禹重实业有限公司为您提供分析仪，有需求可以来电咨询！

SamplePreparationSamplingandsamplepreparationofrefractorymetalssuchastitaniumandzirconiumissomewhatdifferentfromthatofsteel.Unlikesteelsamples,hydrogenisnotasmobileinthisgroupofmaterials;therefore,storageinliquidnitrogenordryiceisnotrequired.However,itisimportanttokeepthesamplecoolwhencuttingorsectioning.Samplepreparationforoxygenandnitrogendeterminationhasbeendifferentfromthatofhydrogendetermination.

Oxygen,Nitrogen,andHydrogeninRefractoryMetalsSummaryOxygenandnitrogenarealloyingelementsintitanium,andarealsoclassifiedasalphastabilizingelementsastheypromotealphaphasealloys.Interstitialoxygenandnitrogenlevelscanbeusedtoregulatethetensilestrengthofthematerial,butduetoitshighsolubilitycancauseunwantedsurfaceembrittlement.Thisphenomenoncanbeleveraged,however,undercontrolledprocessingtocreatesurfacefilmsthatincreasesurfacehardnessandwearproperties.上海禹重实业有限公司致力于提供分析仪，欢迎您的来电哦！

SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.上海禹重实业有限公司是一家专业提供分析仪的公司，有想法的可以来电咨询！温州分析仪供应商

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companyprofileShanghaiUzongIndustrialCo.,Ltd.(hereinafterreferredtoasUZONGLAB®)isahigh-techcompanythatprovidesintegratedsolutionsforintelligentlaboratories,mainlyservingtheChinesemarketandcountriesalongthe“BeltandRoad”.IthasthreebusinessdivisionsandoneThetechnologycenter,namelytheinstrumentbusinessdepartment,consumablesbusinessdepartment,projectdevelopmentdepartment,andZhongyuLianheTechnologyCenter.InadditiontotheShanghaiheadquarters,wehaveestablishedbranchesinBeijing,Shenyang,Shijiazhuang,Taiyuan,Qingdao,Guangzhou,ChengduandUrumqi.Toprovidecustomerswithmoreprofessional,saferandmoreconvenientproductsandservicesisoursolegoal.原装分析仪厂家直销

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