SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.分析仪,就选上海禹重实业有限公司,让您满意,欢迎您的来电!苏州进口分析仪厂家直销
InstrumentHighlightsandFeaturesOptionalFeaturesOptionalboom-mountedtouch-screeninterfacepackage(M)promotesanergonomicworkspaceOptionalPerformancePackage(P)addsathree-stagecarriergaspurificationsystem,andadual-loopgasdosemoduleOptionalDualCoolingPackage(D)addsanintegratedliquid-to-airradiatorwithdualcoolingfans.ThisDCoptiongivestheuserthechoiceofliquid-to-liquidcooling,liquid-to-aircooling,oracombinationofbothOptionalintegratedautocleaner(H)automaticallycleanstheupperelectrodeandlowerelectrodetipOptional20-sampleshuttleloaderavailable泰州力可LECO分析仪上海禹重实业有限公司是一家专业提供分析仪的公司,有需求可以来电咨询!
SummaryThedeterminationoftheamountofoxygen,nitrogen,andhydrogeniniron,steel,nickel-,andcobalt-basealloysrepresentssomeofthemostimportantqualitymetricsforthesematerials.Oxygenisusedtocreatesteelfrompigironbyremovingexcesscarbon.Oxygencontentmustbecontrolledtolimittheamountofcarbonmonoxidethatcanbeformedduringsolidificationwhichmaycauseexcessiveporosity.Nitrogenisconsideredbothanimpurityaswellasanimportantalloyingagent.Itcanbepresentasanitrideorinterstitiallyinitsgaseousform.Increasednitrogencontentisknowntoincreaseyieldandtensilestrength,thusdecreasingductilityandformability.Excessivelevelsmayevolveduringsolidificationthusincreasingporosity.Highhydrogencontentistheprimarycauseofembrittlement,blisteringandflakingduetoitshighmobilitythroughthelatticeandprovidesnopotentialalloyingbenefits.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.
SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.分析仪,就选上海禹重实业有限公司,用户的信赖之选,欢迎您的来电!
氧氮氢分析仪的常见故障及解决方法仪器启动时显示。没有水流。系统分析电流切断,分析停止。这是水流探测器不正常,水泵不工作,管道堵塞。将仪器的右面板取下,观察水流探测器,用手挤压补水塑料水瓶,发现水流正常,显示正常,证明水流探测器正常,管道畅通。启动循环水泵,但分析仪显示没有水流,此时可判定水泵不正常。打开水泵转子密封口,启动泵发现电机正常运转,此时关闭进水,拆下水泵,发现叶轮脱落。经了解,判定是由于外部冷却水停水,仪器内循环水温过高(水温应≤70℃),致使叶轮(叶轮材料PVC)热胀并脱轴。用粘合剂粘合叶轮后再粘于叶轮轴上,待粘合剂凝固后试车,仪器运行正常。分析仪,就选上海禹重实业有限公司,有需要可以联系我司哦!浙江原装分析仪采购
分析仪,就选上海禹重实业有限公司,用户的信赖之选,有需求可以来电咨询!苏州进口分析仪厂家直销
美国LECO力可氧氮氢分析仪ONH836(氧氮氢联测仪)系列硬件部分特点和优势1、炉头区域LED照明系统2、炉头快速拆装的粉尘过滤装置3、装有自动旁路阀的可快速拆装氧水捕集装置4、的动态流量补偿(DFC)保证热导池气体流量、压力恒定5、改进的红外检测池技术 新红外池的恒温绝热技术消除了外界环境温度的干扰 长寿命的红外发射光源和无漂移的电路设计保证红外检测池的长期稳定 氧高低双量程采用3个碳红外检测器,同时检测一氧化碳和二氧化碳,保证准确定量 6、高效脉冲炉冷却系统 强力内循环水冷装置 双直流风扇保证持续冷却,不受电压波动的影响 新电极炉头设计,提高脉冲炉热交换效率 7、全自动分析系统(可选) 自动清扫装置 20位或100位全自动分析系统 高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中,消除环境污染苏州进口分析仪厂家直销
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