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Procedure - Solid Samples

Prepare the instrument as outlined in the operator's instruction manual.

Determine the instrument blank.

Login a minimum of 3 Blank replicates.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Place a 502-344 Nickel Basket into the loading head.

Note: samples using automation should be placed in the appropriate autoloader position before starting the

analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.

Sample Preparation

Sampling and sample preparation is an important issue because traditional methods used to obtain samples for oxygen and nitrogen determination are different from those recommended for hydrogen, especially when sampling molten metal. The main difference in steel sampling procedures for oxygen/nitrogen and hydrogen is due to the mobilityof hydrogen. Special precautions must be used when sampling for hydrogen. From molten steel and iron, a sample must be quickly quenched in cold water and chilled in a refrigerant such as liquefied nitrogen or a mixture of acetone and solid carbon dioxide in order to reduce losses of hydrogen from diffusion. Losses of oxygen and nitrogen from diffusion are not a problem. A sample that is taken for hydrogen and

chilled in a refrigerant can also be used for oxygen and nitrogen determination. However, a sample that is typically taken for oxygen and/or nitrogen determination is not suitable for hydrogen determination due to hydrogen loss (diffusion). Surface contamination must be removed by filing or light grinding, using care not to overheat the sample.

北京专业分析仪厂家直销ONH836仪器通过***采纳客户的反馈意见和创新设计。

company profile

Shanghai Uzong Industrial Co., Ltd. (hereinafter referred to as UZONGLAB®) is a high-tech company that provides integrated solutions for intelligent laboratories, mainly serving the Chinese market and countries along the “Belt and Road”. It has three business divisions and one The technology center, namely the instrument business department, consumables business department, project development department, and Zhongyu Lianhe Technology Center. In addition to the Shanghai headquarters, we have established branches in Beijing, Shenyang, Shijiazhuang, Taiyuan, Qingdao, Guangzhou, Chengdu and Urumqi. To provide customers with more professional, safer and more convenient products and services is our sole goal.

力可ONH836氧氮氢分析仪

特点和优势

国际**的非色散红外及热导检测器 ，无移动部件，不需要手动调整

采用三个**的红外器检测氧含量，同时检测CO和CO2，然后在转化为CO2集中检测，原理上是**完善的，所以不仅可以保证中间量程的测量精度，在**含量和高含量的检测范围内同样可以满足精度要求

高性能的红外检测器配置***恒温绝热技术，消除了外界环境温度的干扰

长寿命的红外发射光源和无漂移的电路设计保证检测器的长期稳定性

力可**的动态流量补偿控制DFC系统，保证了流量系统的完善，可以精确控制整个气路中的流量，保持流量恒定**改善了材料中氮分析的准确度

可以旁路的OMI-2 气路强化过滤装置增强了检测器的稳定性，使得分析结果更加准确

可选自动功能

20位试样自动进样系统

通用下电极坩埚支座，容纳各种坩埚使用

无需人工干预的全自动清扫系统

采用三个**的红外器检测氧含量，同时检测CO和CO2，然后在转化为CO2集中检测。

Procedure - Solid Samples

Instrument calibration/drift correction.

Place the calibration/drift standard in a *** Nickel Basket, and if applicable, place the sample into the appropriate autoloader position.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

Note: samples using automation should be placed in the appropriate autoloader position before starting the

analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.

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Method Selection

Two methods are described in this application note; either method can be used to analyze iron, steel, nickel-, and cobalt-base alloys. The Precision Method is recommended for general use and will provide the best precision and accuracy throughout the typical O, N, and H concentrations found in this group of metals; approximate cycle time is 3.5 minutes. The Fast Track method can be used where speed of analysis is a critical component; for example, when molten metal is being sampled and results are required in the shortest possible time. This method will produce suitable results for most samples; approximate cycle time is 2.25 minutes. As noted above, sampling and sample preparation are key elements to accurate O, N, and Hdetermination as well. It is up to the user to determine which method best meets their needs.

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